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Re: Thermocouple gauge
Looks like you got a toy to play with; seems like toys can be found on Ebay for cheap. At least you got a very good laboratory vacuum pump for cheap. I don't know enough about them to know what I would be buying; but as I understand it you don't have to worry about back streaming from it. As for me I have purchased diffusion pumps for very cheap; but without any baffle. So far baffles on Ebay are too expensive; hence I am considering making something that will reduce back streaming. From: Thomas To: VacuumX@... Sent: Wednesday, February 20, 2013 5:12 PM Subject: [VacuumX] Re: Thermocouple gauge
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Vaughn:
Can't answer your question as well a most of the guys in this group. Just wanted to say that I too grew up on C.L. Stong and 60's era Vacuum. I recently purchased on Ebay a good Turbo Pump and controller for a crazy low price. I thought I might have to at least replace the bearings, but, it revs up just fine. Tom M. --- In VacuumX@..., "Vaughn Mcdowell" wrote: > > I am a baby boomer retired in my late 60's. When I was in high school I was experimenting with refrigerator rotary pumps as described by Strong in the Amateur Scientist articles. As a senior in high school I learned to blow Pyrex glass; during college in undergraduate and graduate I worked with vacuums systems but mostly for building Argon ion and N2 lasers. I did some diffusion pump work but very briefly. I remember using gum rubber tubing, stop cock valves, and Pyrex glass tube connections. Afterward I haven't touched vacuum systems until 2003 ( fired up my diffusion pump) but very briefly; and recently much more. I have always had a love for vacuum systems. But my vacuum world has changed significantly with quick disconnect etc. I feel like Rip Van.. Having limited funding I looked to Ebay for getting components that I could afford. I have been slowly acquiring KF fittings for future use. In the meantime I am using what I know to get by with. "Procedures in Experimental Physics " Strong has been my Bible. I have acquired more recent Varian training manuals; info from Bell Jar; etc. > > When I was in College McLeod gauges were used for reference; now I have very limited vacuum references; the gas discharge method; the TC gauge and Ion gauge method. The first method is very dangerous in the 10 micron and below: http://vaughns_page.50webs.com/vacuum/gas_discharge1/X-ray1/x-ray_gas_tube1.html > > I have abandoned this method; in the future I have some high voltage experiments in mind: http://vaughns_page.50webs.com/vacuum/magnetron/9Jan13Exp/9jan13Exp.pdf . > > The TC gauge is limited but I am mainly interested in some ball park idea; I have purchased several DV-6M types new and used; I can used the hysteresis factory data to get some reference but how do I know if is new that some oil back streaming hasn't changed or shifted the thermodynamic continuity flow equilibrium much less the non linear characteristics? When I started testing my diffusion pumps the TC controller would quickly peg below zero; I started zeroing my TC controllers using the diffusion pumps. At the moment I feel like I am working in the dark. Even if I were to use a calibrated TC gauge; how do I know mechanical and diffusion pump back streaming won't significantly affect its thermodynamics significantly?? > > Thanks > |
Re: Thermocouple gauge
¿ªÔÆÌåÓýThomas wrote: ???? Me too.? I still have some stuff I bought from Frank Lee including a couple of the little single-stage oil pumps, one unused.? I've had a lot of fun with them. Ed
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Re: Thermocouple gauge
Vaughn:
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Can't answer your question as well a most of the guys in this group. Just wanted to say that I too grew up on C.L. Stong and 60's era Vacuum. I recently purchased on Ebay a good Turbo Pump and controller for a crazy low price. I thought I might have to at least replace the bearings, but, it revs up just fine. Tom M. --- In VacuumX@..., "Vaughn Mcdowell" <vaughn.mcdowell@...> wrote:
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Re: Vacuum
¿ªÔÆÌåÓýWe get normally get good results after plasma cleaning if we get anything below 1.0e-4 Torr. We coat a few mirrors a month. This time we could not get below 1.7e-4 torr. Guy On Feb 17, 2013, at 18:23, Vladimir Chutko <chutko@...> wrote:
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Re: Vacuum
Guy,
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Al coating performance strongly depends on vacuum and deposition rate. In general, it is recommended to evaporate Al on a cold substrate at pressures at least below 2x10-5 torr with deposition rate at least 10 A/s. Othervice the growing coating will trap air molecules, adhesion and mechanical properties will be not good, and you won't be able to obtain really high reflectance. The substrate pre-cleaning with an ion beam or glow discharge is also needed. Regards, Vladimir Chutko On 2/12/2013 6:55 PM, Guy Brandenburg wrote:
Just tried and failed to aluminize a mirror because the pressure would not go below 1.7x10^-4 torr; as a result the coating was semi transparent. If it goes below 1.0e-4 all is good. This is unusual. Persisted even when i tightened stuff up.------------------------------------ |
Re: Veeco EP 2A 1 DP backed by 1402
¿ªÔÆÌåÓýThanks for sharing Vaughn, nice setup. I'm also learning and gathering equipment. I have a gauge controller that I can't find any information about and will have to reverse engineer it to use. Can you give me the links to the manual and schematics for your controller (or email it to me) as it will help me understand mine a bit better please.I look forward to seeing your progress. Don Black. On 18-Feb-13 5:44 AM, Vaughn Mcdowell wrote: ? |
Veeco EP 2A 1 DP backed by 1402
I decided to test my Veeco diffusion pump using the 1402 that I have just refurbished. At the present I am using my Web site for documenting my experiments, which I don't mind sharing; it is very convenient for me; decided to share photos of my experimental setup.
The following link shows a photo of the 1402 backing the DP: I don't have yet any 2" vacuum pluming; attached to the top is a quick adapter for the TC and ion gauge tube to sample the pressure. I plan to have something more suitable in the future. The ion gauge should be rotated 90 degrees; the tungsten heater is drooping slightly which I understand affects its sensitivity value. The next link shows the TC gauge that was zeroed after the DP reached 0.1 micron. The next link shows the CVC ion gauge controller; The emission current is 1 ma. corresponding to slightly higher than 0.02 micron reading. At 10 ma. the pressure settles to about 0.06 micron; as expected higher than that at 1 ma. I believe this is due to enhanced electron space charge cloud. I got two of these for very cheap; I wanted something very basic to learn from; I was able to fine the manual with schematics on the Web; before using, the emission current and electrometer were checked ( using my DVMs) for calibration. I was very surprised after so many years how close to calibration they were. The last link shows the DP that I modified for the cooling fan I found in my junk box: Having no information regarding this DP; I decided to try using about 70 cc of the Specialty Fluid 704 equivalent ( at the time it was the cheapest that I could find); The Variac, for the heater, was finally set to 100 VAC corresponding to the above results; don't know for the this fluid type what the optimum Variac setting should be. Regarding the ion gauge reading ( 1 ma. emission) assuming the typical sensitivity value given for ( N2 or air). I do know that I started with air; however what I don't know is what the ion gauge is ionizing ( out gas ; back streaming etc); Out gassing in the ion gauge itself; I didn't do much degassing yet. I don't know typically how close to the typical sensitivity value given should be trusted. I am a novice getting my feet wet just learning how to drive. My goal is to eventually get down near 10-6 Torr someday for electron beam experiments that I have in mind. |
Thermocouple gauge
I am a baby boomer retired in my late 60's. When I was in high school I was experimenting with refrigerator rotary pumps as described by Strong in the Amateur Scientist articles. As a senior in high school I learned to blow Pyrex glass; during college in undergraduate and graduate I worked with vacuums systems but mostly for building Argon ion and N2 lasers. I did some diffusion pump work but very briefly. I remember using gum rubber tubing, stop cock valves, and Pyrex glass tube connections. Afterward I haven't touched vacuum systems until 2003 ( fired up my diffusion pump) but very briefly; and recently much more. I have always had a love for vacuum systems. But my vacuum world has changed significantly with quick disconnect etc. I feel like Rip Van.. Having limited funding I looked to Ebay for getting components that I could afford. I have been slowly acquiring KF fittings for future use. In the meantime I am using what I know to get by with. "Procedures in Experimental Physics " Strong has been my Bible. I have acquired more recent Varian training manuals; info from Bell Jar; etc.
When I was in College McLeod gauges were used for reference; now I have very limited vacuum references; the gas discharge method; the TC gauge and Ion gauge method. The first method is very dangerous in the 10 micron and below: I have abandoned this method; in the future I have some high voltage experiments in mind: . The TC gauge is limited but I am mainly interested in some ball park idea; I have purchased several DV-6M types new and used; I can used the hysteresis factory data to get some reference but how do I know if is new that some oil back streaming hasn't changed or shifted the thermodynamic continuity flow equilibrium much less the non linear characteristics? When I started testing my diffusion pumps the TC controller would quickly peg below zero; I started zeroing my TC controllers using the diffusion pumps. At the moment I feel like I am working in the dark. Even if I were to use a calibrated TC gauge; how do I know mechanical and diffusion pump back streaming won't significantly affect its thermodynamics significantly?? Thanks |
Re: Tri Clover Fittings
¿ªÔÆÌåÓýHowdy,Sigh...you're right. Here's a high-res photo of some gaskets: They look mainly flat, with a ridged part around them, and the flanges have an O-ring groove in them. I suppose the advantage of that is you don't need a centering ring like with KF flanges. You can get Buna-N (nitrile) gaskets easily, and fortunately some sites (found one EBay store ) sell Viton gaskets. Could be, although I would've thought that for hygienic reasons they'd ensure there's no places where stuff could get trapped or porosity. The large flat gaskets might give rise to this. Would be very interested to hear how it goes! It turns out I can get them in the UK, just searching under "tri clamp fitting" instead. On a related hardware topic, have you ever come across the convoluted metal hose used for domestic gas main installations? Stuff like this - Maybe things are different in the US, but there's always a bit of that stuff used between the gas main and house regulator. It looks to be very nice for vacuum use - not quite as flexible as proper vacuum bellows tubing, but still pretty good. Also see ebay for "flexible exhaust" - for example item 230830064598. Again, bellows tubing just like that used for vacuum. No ends unfortunately! Cheers, Lindsay
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Re: Tri Clover Fittings
¿ªÔÆÌåÓýPlease keep us informed of what you find, they do seem a fraction of the price of "proper" vacuum fittings. You make good points about trapped volume leaks and seals though. Hope they work out. The maximum temperature of "rubber" seals, O-rings, etc. is important for baking out too.Don Black. On 16-Feb-13 3:26 AM, Gomez Addams wrote: ? |
Re: Welch 1402
Or thermite when mixed with aluminum powder...also not good for your vac pump! On Wed, Feb 13, 2013 at 5:53 PM, Gomez Addams <gomez@...> wrote:
-- Nick A "You know what I wish?? I wish that all the scum of the world had but a single throat, and I had my hands about it..."? Rorschach, 1975 "They that can give up essential liberty to obtain a little temporary safety deserve neither liberty nor safety."- Benjamin Franklin, Historical Review of Pennsylvania, 1759 "Suburbia is where the developer bulldozes out the trees, then names the streets after them." Bill Vaughan "The price of apathy towards public affairs is to be ruled by evil men." Plato |
Re: Tri Clover Fittings
Gomez Addams
On Feb 15, 2013, at 3:53 AM, imajeenyus42 wrote:
Howdy,The first issue I foresee is the o-ring material. If the seals are standard O-rings, great, then you can just order Viton O-rings. But I thought those fittings used custom seals with odd cross-sections. Another possibility to think about is that they don't have to be absolutely gas-tight for dairy operations, small leaks may be permitted. Another thing to think about: for the most part, high vacuum fittings are designed such that when assembled together, very little "trapped" volume remains in the conjoined system, that is, space that is connected to the pumped volume, but has low conductance, IOW, "nooks and crannies". But I agree that these do resemble KFs an awful lot, and I'm going to start comparing prices out of curiosity - if they are drastically cheaper than what I can get from Duniway et al, then an experimental purchase and test would seem in order! - Bill "Gomez" Lemieux, The Highland Tinker |
Re: Welch 1402
Gomez Addams
On the gasket where the case parts split - is that RTV?
There's no chance any RTV got inside the pump or any oil-wetted surfaces is there? I'm probably stating the obvious, but I don't think you want an aromatic acid like acetic any where in your vacuum system, for both obvious reasons. OTOH, if you've flushed the pump and its backing a DP well, that would sorta prove the pudding, I suppose. :) - G. On Feb 14, 2013, at 3:25 PM, Vaughn Mcdowell wrote:
- Bill "Gomez" Lemieux, The Highland Tinker |
Tri Clover Fittings
Howdy,
I've been a lurker here for some time - came across this recently and thought it might be interesting/useful. While looking for some info on brewing, I found these "tri clover fittings": They seem to be standard in brewing/dairy plant, and look very similar to the KF vacuum fittings (genderless flanges, O-ring, and clamp). They're polished for hygenic reasons, so I guess would do well for vacuum. Most importantly they're dirt cheap! Maybe you know about them already, but they're totally new to me (in the UK, where we seem to be behind the times....) Incidentally, no relation to the "tri laser connector" that Bones used to fix Spock's brain ;-) Cheers, Lindsay |
Re: Welch 1402
After I have put new oil in my pump ; it was tested again; it has been partially repainted ; added intake and exhaust? components; decided to give links of my Web showing photos of my new toy and TC gauge measurements. I don't plan to do anything more on it; plan to using it for testing my largest diffusion pump. The TC gauge reading is shown: http://vaughns_page.50webs.com/vacuum/1402Ebay_2/100_1684b.JPG When I initially got this gauge from Ebay and tested it with one of my diffusion pumps; the needle pegged well below ? zero very quickly after warming up. After running for some time the controller? was adjusted so that the needle was set to zero. Although the 1402 seems to pump fairly quickly at first; it takes quite a long time for it to reach the value indicated. I am not claiming that the TC value is absolutely correct ; just what it reads after being zeroed with a diffusion pump. Photos of the 1402 that I refurbished : http://vaughns_page.50webs.com/vacuum/1402Ebay_2/100_1678c.JPG http://vaughns_page.50webs.com/vacuum/1402Ebay_2/100_1678c.JPG I am happy with my new toy |
Re: Welch 1402
Gomez Addams
Yeah, you can't use anything even slightly abrasives to remove rust
from any of the bearing/wiping/sliding surfaces such as shafts and vanes and valve seats and so forth. If there is pitting or a change in the shape or surface quality of the cleaned steel, that part is scrap. On Feb 14, 2013, at 5:22 AM, Russell Shaw wrote: On 14/02/13 02:36, Vaughn Mcdowell wrote: - Bill "Gomez" Lemieux, The Highland Tinker |
Re: Welch 1402
On 14/02/13 02:36, Vaughn Mcdowell wrote:
... Regarding freeze up besides rust rotor and stator components keeping then fromFor rust-removal, evaporust is good because it dissolves rust instead of converting it like other stuff. It works better when warm > 20-25degC. Complete immersion or continuous spraying with a jet is best. The 1402 that I recently got on Ebay didn't have exhaust or air intakeYou could make an oil mist output filter using a car oil or air filter. |
Re: Welch 1402
Gomez Addams
I worked for an outfit who bought consumables and hardware from Duniway on a regular
basis. Their staff are knowledgeable - at least the ones I spoke to - and they do not sell junk, as far as I can tell. No vacuum vendor will survive long selling lousy stuff, the market is too small. Duniway has the best prices I've found anywhere, and I've had no trouble with anything I've bought from them for my personal use. I think I might worry a little bit about dual-use oil, until I know more about it. It seems to me just a little hard to believe that an oil good for DP operation will also have sufficient high-pressure lubricity to preserve the bearing surfaces in my mechanical backing pump. I admit to ignorance, but the requirements for the two applications are so different - with the exception of possessing low vapor pressure when cold, obviously, that it just seems wiser to me to use what the manufacturer's recommend: DP oil in the DP, mechanical oil in the mechanical pump. On Feb 13, 2013, at 8:36 AM, Vaughn Mcdowell wrote: It seems that vacuum pump oil price has gone up recently; for awhile I have been purchasing , from Specialty Fluids Co. their type MVT-20 which is apparently a hydrocarbon dual use ( diffusion and mechanical). I have had good experience using it. I am considering their MVT-19 which costs less. I have also started using the INLAND 19 TOP QUALITY HIGH VACUUM PUMP OIL ; its in my opinion very good . However I must confess my vacuum experience is very limited; I am in the learning mode. I am hoping to look into Duniway to see if it is a better fit to the beer budget. - Bill "Gomez" Lemieux, The Highland Tinker |