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aluminizing chamber electrodes queery
This is my first post to this list. Let's see if it works.
I have a vacuum chamber, which pulls needed vacuum for aluminizing, so I am now at stage of needing to get electrodes into the stainless steel chamber. James Learch already offered some ideas, and I was hoping to see if there were others as well. I would be happy to know of specific electrodes used and how they were inserted into the chamber. Along same line, anyone know if Tungsten is really required? Can I now instead use something like Kanthal wire or perhaps a car cigarette lighter heating element, etc? This seems more convenient. I'll now wait and see if this gets distributed to the members. Dominic-Luc Webb |
Darald Bantel
Greetings
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I have NO experience with vacuum coating - but I would think that your car cigarette lighter element would more likely be a nichrome type of wire. From the Kanthal website it is rated to 1450 degrees C and nichrome may be rated higher (but I doubt it) whereas tungsten is rated at over 3400 degrees C - I know which one I would be using! Darald On Mon, 2003-12-08 at 03:38, Dominic-Luc Webb wrote:
This is my first post to this list. Let's see if it works. |
Tungsten is strong for its thickness, but generally is very, very
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thin, as in light bulbs. However, the nichrome and kanthal wires are commonly much thick so are quite strong. Reduced form of aluminum goes to melts at slightly above 500 degrees. It is not clear to me that the temperature ratings you mention are the determining factor in choice. I rather like the strength of highly re-usable things like car cigarette lighters and kanthal wires. Perhaps there are specific tungsten electrodes one would suggest? Perhaps someone knows there is in fact a reason to not use these other options? Dominic-Luc Webb On Mon, 8 Dec 2003, Darald Bantel wrote:
Greetings |
Gomez
On Monday, December 8, 2003, at 07:31 AM, Dominic-Luc Webb wrote:
Tungsten is strong for its thickness, but generally is very, veryTry TIG welding electrodes. However, the nichrome and kanthal wiresThe issue is whether one wishes to evaporate pure aluminum, or also evaporate aluminum and some of your heating element with it, contaminating your mirror coating. Tungsten's extremely low vapor pressure even at high temperatures makes this very unlikely. The same cannot be said for Nichrome. I don't know what is in Kanthal and I'm too lazy to Google for it, but I do know you don't want to sputter your mirror with nickel (an ingredient of nichrome). |
arcstarter
--- In VacuumX@..., Dominic-Luc Webb <dlwebb@c...> wrote:
On Mon, 8 Dec 2003, Gomez wrote:I think that if have decided to wind your own W filaments - youTry TIG welding electrodes. would be better off buying wire from www.smallparts.com as recently posted. Now about welding rods. Your welding supplier will carry all sorts of TIG welding electrodes. Typically the pure tungsten rods will have a green end (paint), and are used for TIG welding aluminum. Other types are 2% thoriated as well as types including other rare earch alloying ingredients. These ingredients increase electron emission during the welding proces, but are probably not wanted for evaporation. Last time I bought abox of 0.020 inch rods price was about $12 for 10 rods. 6 inches long. As someone has pointed out they are brittle unless properly warmed. I would think that bulk wire purchased from smallparts would't have this problem (but I could be wrong). Lesker.com carries all sizes and shapes of pre-spiraled tungsten filaments. -Bill Dominic-Luc Webb |
James Lerch
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----- Original Message -----
From: "arcstarter" <arcstarter@...> Last time I bought abox of 0.020 inch rods price was about $12 forThe bulk wire is just as brittle has the Tig electrodes :0 I still find it pretty amazing that a material with such a high melting point, has a Brittle to Ductile transition temperature starting as low as 100C. Take Care, James Lerch (My telescope construction,testing, and coating site) "Anything that can happen, will happen" -Stephen Pollock from: "Particle Physics for Non-Physicists: A Tour of the Microcosmos" |
Gomez
On Monday, December 8, 2003, at 11:29 AM, Dominic-Luc Webb wrote:
On Mon, 8 Dec 2003, Gomez wrote:So far as I know, they are all Tungsten. Some are alloyed with a small amount of Thorium, which makes the arc easier to start. I assume we don't want that.Try TIG welding electrodes. |
¿ªÔÆÌåÓýYou may recheck your Kanthal catalog as nichrome may be good for 1450 F as compared to C. A cigarette lighter will vaporize the aluminum but then you will alloy the aluminum with the nichrome and decrease it's life as a heating element considerably.. A relatively cheap source of tungsten is an electrode for a TIG welder (TIG...Tungsten Inert Gas ) it is a very stiff wire about 6" long of various diameters under 1/8". A beer can which is 99.9% Al. bent over the tungsten will vaporize enough Al. to coat most mirrors.
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Bill Lang |
Hello All,
? In my experince of vacuum coating, we should use tungsten filament for evaporating the aluminum.
Ismail
Darald Bantel wrote: Greetings Do you Yahoo!? |
On Mon, 8 Dec 2003, Gomez wrote:
Not knowing welding, are all TIG electrodes tungsten, or shouldSo far as I know, they are all Tungsten. Some are alloyed with a OK, I looked around on the Net and did some quick learning about TIG electrodes. As one member already suggested, green does appear the best choice, being essentially pure tungsten (99.97%). This type has letter symbol designations such W, WP, YWP and EWP, but all are color coded green. Other types have small traces of La, Th, Zr or Ce and have their respective character designations indicate the added metal, like EWCe or EWLa, etc. Even these are 97-99.3 tungsten. Interestingly, while TIG electrodes seem to be more expensive over here in Sweden (5 USD each), they are a lot longer, typically 300 mm, about 12" US units. Here is the link to a place that has a decent-looking table of codes and compositions for TIG electrodes: Dominic-Luc Webb |
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