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Re: aluminizing chamber electrodes queery

Darald Bantel
 

Greetings

I have NO experience with vacuum coating - but I would think that your
car cigarette lighter element would more likely be a nichrome type of
wire. From the Kanthal website it is rated to 1450 degrees C and
nichrome may be rated higher (but I doubt it) whereas tungsten is rated
at over 3400 degrees C - I know which one I would be using!

Darald

On Mon, 2003-12-08 at 03:38, Dominic-Luc Webb wrote:
This is my first post to this list. Let's see if it works.

I have a vacuum chamber, which pulls needed vacuum for aluminizing,
so I am now at stage of needing to get electrodes into the stainless
steel chamber. James Learch already offered some ideas, and I was
hoping to see if there were others as well. I would be happy to
know of specific electrodes used and how they were inserted into
the chamber.

Along same line, anyone know if Tungsten is really required? Can I
now instead use something like Kanthal wire or perhaps a car cigarette
lighter heating element, etc? This seems more convenient.

I'll now wait and see if this gets distributed to the members.

Dominic-Luc Webb





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aluminizing chamber electrodes queery

 

This is my first post to this list. Let's see if it works.

I have a vacuum chamber, which pulls needed vacuum for aluminizing,
so I am now at stage of needing to get electrodes into the stainless
steel chamber. James Learch already offered some ideas, and I was
hoping to see if there were others as well. I would be happy to
know of specific electrodes used and how they were inserted into
the chamber.

Along same line, anyone know if Tungsten is really required? Can I
now instead use something like Kanthal wire or perhaps a car cigarette
lighter heating element, etc? This seems more convenient.

I'll now wait and see if this gets distributed to the members.

Dominic-Luc Webb


Re: ATM book 3 article on telescope mirror coating

 

--- Gomez <gomez@...> wrote:
On Friday, November 21, 2003, at 07:18 AM,
gjnelson@...
wrote:

I have scanned a copy of the article on
aluminising telescope mirrors
from amateur
telescope making book 3. It is a large 1.2 Mb
file. If anyone would
like me to email
them the pdf I am willing to do so.
Amigo Gomez:
I take your offert of the copy of the article on
aluminsing telescope mirrors.
I garantee you, it is for my personal use only.
Plese mail me the pdf.
Tanks you.

=====
Alberto Gasparini
Perito Moreno 1032
Godoy Cruz (5501)
Mendoza
ARGENTINA
telefono 0261-422-0923

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Re: Evaporator

arcstarter
 

Well I have the 1397 running. Ran a few fluid changes through it to
displace the nasty old oil and water. Haven't plumbed it all
together but it sure appears to pull quite a bit of air.

Also received an order of tungsten boats and a new TC gauge.
Shouldn't be too long before I have it running.

-Bill

--- In VacuumX@..., "Ken Hunter" <atm_ken_hunter@y...>
wrote:
Good find! That 1397 will suck all the air out of a 10 inch diff
pump
in short order.. If you have a smaller diff pump it's overkill but
you'll sure be able to recycle quickly!

Ken Hunter


Re: Evaporator

Ken Hunter
 

Good find! That 1397 will suck all the air out of a 10 inch diff pump
in short order.. If you have a smaller diff pump it's overkill but
you'll sure be able to recycle quickly!

Ken Hunter


--- In VacuumX@..., "arcstarter" <arcstarter@y...> wrote:
Guys,
I recently purchased a used (and abused) evaporator, and am in the
process of refurbing the same.

If anyone cares I can probably post pictures and more information
on the specific machine. Belljar is 12 inch diam 18 inches tall.
Dual tungsten/Moly boats. Used in production service for the
evaporation of nickel, silver, and gold for quartz crystal
construction.

Machine came w/o vacuum pumps but I have since located a Welch
1397
mechanical pump and a small diffusion pump.

-Bill


Evaporator

arcstarter
 

Guys,
I recently purchased a used (and abused) evaporator, and am in the
process of refurbing the same.

If anyone cares I can probably post pictures and more information
on the specific machine. Belljar is 12 inch diam 18 inches tall.
Dual tungsten/Moly boats. Used in production service for the
evaporation of nickel, silver, and gold for quartz crystal
construction.

Machine came w/o vacuum pumps but I have since located a Welch 1397
mechanical pump and a small diffusion pump.

-Bill


Re: ATM book 3 article on telescope mirror coating

Gomez
 

On Friday, November 21, 2003, at 07:18 AM, gjnelson@... wrote:

I have scanned a copy of the article on aluminising telescope mirrors from amateur
telescope making book 3. It is a large 1.2 Mb file. If anyone would like me to email
them the pdf I am willing to do so. Please note copyright does exist on this article and I
am only making this offer for people who do not have access to the original. I know
Willmann-Bell do still publish the full series and it would be better to buy the books. So
far as I understand making a copy of a limited amount of a published work is legal as
long as it is for personal use.

Somebody please correct me if I am wrong and I will retract the offer.
Not that I am a stickler for adhering to every single law (just some of them), but you seemed to want to know:

Generally speaking, copyright law allows you to make a copy of a work which you have purchased, for your own personal use. However, "personal use" does not include distributing copies to others.


Re: ATM book 3 article on telescope mirror coating

 

Geoff,


You might want to compare it to: 2. W. Kindred, J.T. Williams, and D. Clark, "In situ Aluminization of the MMT 6.5 m Primary Mirror," MMTO Technical Report #03-8, (June 2003); also www.mmto.org/MMTpapers/pdfs/tm/tm03-8.pdf .

If your article has some interesting information I would appreciate a copy at donmattox@...

Many thanks

Don?


Hi

I have scanned a copy of the article on aluminising telescope mirrors from amateur
telescope making book 3. It is a large 1.2 Mb file. If anyone would like me to email
them the pdf I am willing to do so. Please note copyright does exist on this article and I
am only making this offer for people who do not have access to the original. I know
Willmann-Bell do still publish the full series and it would be better to buy the books. So
far as I understand making a copy of a limited amount of a published work is legal as
long as it is for personal use.

Somebody please correct me if I am wrong and I will retract the offer.

Kind regards
Geoff

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-- 
____________________________________
Donald M. Mattox
Technical Director
Society of Vacuum Coaters
71 Pinon Hill Place NE
Albuquerque, NM? 87122-1914

Telephone 505/856-7188
FAX 505/856-6716
E-mail donmattox@...
WebSite? http://www.svc.org


ATM book 3 article on telescope mirror coating

 

Hi

I have scanned a copy of the article on aluminising telescope mirrors from amateur
telescope making book 3. It is a large 1.2 Mb file. If anyone would like me to email
them the pdf I am willing to do so. Please note copyright does exist on this article and I
am only making this offer for people who do not have access to the original. I know
Willmann-Bell do still publish the full series and it would be better to buy the books. So
far as I understand making a copy of a limited amount of a published work is legal as
long as it is for personal use.

Somebody please correct me if I am wrong and I will retract the offer.

Kind regards
Geoff


ATM book 3 article on telescope mirror coating

 

Hi

I have scanned a copy of the article on aluminising telescope mirrors from amateur
telescope making book 3. It is a large 1.2 Mb file. If anyone would like me to email
them the pdf I am willing to do so. Please note copyright does exist on this article and I
am only making this offer for people who do not have access to the original. I know
Willmann-Bell do still publish the full series and it would be better to buy the books. So
far as I understand making a copy of a limited amount of a published work is legal as
long as it is for personal use.

Somebody please correct me if I am wrong and I will retract the offer.

Kind regards
Geoff


ATM book 3 article on telescope mirror coating

 

Hi

I have scanned a copy of the article on aluminising telescope mirrors from amateur
telescope making book 3. It is a large 1.2 Mb file. If anyone would like me to email
them the pdf I am willing to do so. Please note copyright does exist on this article and I
am only making this offer for people who do not have access to the original. I know
Willmann-Bell do still publish the full series and it would be better to buy the books. So
far as I understand making a copy of a limited amount of a published work is legal as
long as it is for personal use.

Somebody please correct me if I am wrong and I will retract the offer.

Kind regards
Geoff


Stolen Scope

Ken Hunter
 

STOLEN:

A StarMaster 30" telescope w/ an Argo Navis DSC and a White 17'
Haulmark "V" nose, tandem wheel trailer which has a ramp rear door
and a 36" side door on the right. Items were taken from my residence
in Albuquerque, New Mexico in the early morning on Thursday, 13
November, 2003. Also included in the trailer was a Craftsman brand
tool cabinet that contained hand tools of approximately $1500 value,
and two 10 ft Tripod ladders (Louisville red fiberglass and Tallman
aluminum).

Any information on the whereabouts of these items would be greatly
appreciated. Please contact the Albuquerque Police Department. In
addition, the owner, Brock Parker can be reached at (505) 298-2792 or
E-mail starbadger203@y... or Additional Contact: Sammy Lockwood
(505) 275-0258 or E-mail brock@s...

Brock B. Parker AKA (a brokenhearted) starbadger
-----------------------------------------------------
Brock has registered his loss with Starmaster, Argo Navis, and
several other astronomically related sites. Our theory is that crack-
heads or similar low-life's stole the trailer without knowing it's
contents, and will likely either trash it's unusual contents, or
hopefully, try to sell it. Apparently, his insurance will not cover
this loss.

Obviously, the only hope to reclaim this scope is to get the word out
as far and wide as possible. There are only 6 scopes like this in
existence, so maybe we'll get lucky. I would ask that you forward
this note to any/all astronomical listservs and bbs's. Ff possible,
link to your post to www.taas.org/stolen_starmaster/, where a
picture and info are available.

If there is any good news here, it's that his 18" dob, and his
eyepiece case was not in the trailer.


Re: More questions about oil diffusion pumps

 

Mr. Peter John Smith:
After looking your reprints of diffusion pumps, I can
see all of them have ejector as the last stage.
I wish to know where are the benefits of the ejector
system and also the problems it can bring.
Do you have a close drawing of the ejector, with
dimensions and critical details.
I am glad you are all ears, if anyone else has more
info on actual dimensions and construction of a diff
pump.
Thanks you.
Albert Gasparini

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Re: More questions about oil diffusion pumps

 

It would be an option but the transport cost to SA makes any option on ebay out of my
current budget. Otherwise I most likely would be in business now.

I was just going to run without valves. Good baffles and hope like hell the power does
not go out. I will switch off the pump let it cool and then let the atmosphere in. Cycle
time per item in the chamber will be longer but it is the only current option with out
spending more money than I have.

Geoff

Check out E-bay for old diff. pumps there are a couple there now with
traps, valves and one with a gauge controller and gauges. you can make
a pump but it is probably cheaper to buy one, the valves are a big
buck item that is hard to make. Hopefully I'll get a chance to sketch
up mine this week end.

Ron White



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Re: More questions about oil diffusion pumps

 



Geoff,

Check out E-bay for old diff. pumps there are a couple there now with traps, valves and one with a gauge controller and gauges. you can make a pump but it is probably cheaper to buy one, the valves are a big buck item that is hard to make. Hopefully I'll get a chance to sketch up mine this week end.

Ron White


Duniway's "Pentavac 5" DP oil

Gomez
 

Has anyone used it? In their latest paper catalog, which arrived in the mail yesterday, Duniway claims that it has higher oxidization resistance, higher operating temperature limits, and lower vapor pressure at elevated temperatures than any other DP (diff. pump) fluid, including the exotic silicones such as Fomblin. They claim you can even expose the DP to atmosphere (they did it repeatedly in tests) without harm to fluid or pump. (!) They claim its back-streaming rate is so low that in most applications, a cold trap is not necessary. (!)

All of this seems too good to be true, but if true, it's a wonder product.

So, has anyone used it? It's hideously expensive, $130 for 100cc's, which puts it in the same class as the exotic silicone DP fluids, but if all their claims are true, it would be worth it.

- Bill "Gomez" Lemieux

.........................
186,000 miles per second.
It's not a good idea,
it's just the law.


Re: More questions about oil diffusion pumps

 

Geoff,

Take a look at http://209.210.231.220/Vacuum/Technique/Vacuum3.html for some ideas about how the pumps work.

Don Mattox
Peter John Smith put a picture on his website of the internal construction of a vacuum
pump. It has helped but I don't think I understand and the drawing is not clear enough. I
also had a really good look at the picture of the glass pump. Please correct me if I am
using incorrect terminology.

Now for the questions.

How critical are the tolerances of the jet openings? The glass pump seems to have
quite big openings. Are the angles exceptionally critical? perpendicular will not work. I
assume that the angle has to be in the direction of flow as much as possible

How is the oil kept out of the pipe to the roughing pump? Or possibly a better question
is; how is the internal connection to the roughing pump normally made? The rough
drawing that the glass blower showed me had a collection chamber fed by a pipe to the
vaporisation chamber that sat below it. The glass pump picture just shows a pipe
exiting the chamber with possibly a connection to the lowest jet.

How does a fractionating pump work. Is it just the height of the assembly as is normally
done with fractional distillation? Which means any pump with jets at different heights
will be a fractionating pump.

Does the whole jet assembly fit in the body loosely or is it secured in?

Are each of the jets fed separately or are all the jets fed from the same tube? The glass
pump seems as if all are fed separately but the pump Peter John Smith showed seems
to have one tube. Is this the difference between a fractionating and non fractionating
pump?

I am sure I will think of some more questions to ask but I'll give you guys a break for
now.

Thanks

Geoff

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-- 
____________________________________
Donald M. Mattox
Technical Director
Society of Vacuum Coaters
71 Pinon Hill Place NE
Albuquerque, NM? 87122-1914

Telephone 505/856-7188
FAX 505/856-6716
E-mail donmattox@...
WebSite? http://www.svc.org


Re: More questions about oil diffusion pumps

 

¿ªÔÆÌåÓý

I have put 4 more scans on my web pages with info about Diff Pumps.
?
These are from the quite old book - 1947 to be precise.
?
A Manual of Vacuum practice by Martin and Hill.? This has been reprinted by Lindsay Publications.
?
?
?
?
?
I dont think these represent the latest thinking but the pages of text and diagrams explain the idea of a Diff Pump with combined Fractionating in the evaporating chamber.? The original one I uploaded is far more modern.
?
The two top gaps in these latest pics are 3/32 inch - they did not copy too well.? All other dimensions are readable.
?
I doubt that the fractionating function is necessary with good pump oils unless you are after really high vacuum.? Essentially, the oil is returned to the outermost portion of the base chamber.? The oil is in semiseperated annular portions - each supplying vapor to different nozzles in the diff pump.? The central evaporating portion supplies oil vapor to the top nozzle.? For oil to be returned to the inner part, it must first pass through the outer and middle chambers by passing through slots.? These are arranges so they are on different sides so there is a totturous path for the oil.? The idea is that by the time it returns to the centre, the more volatile fractions are evaporated away.
?
Although I have little actual figures, from all I have read, the nozzle shapes and dimensions are not all that critical unless you want absolute maximum pumping speed and the ability to work at the highest pressure.? The early pumps were crude and , although they were slower, they did work.? The first pump really did not have a nozzle as we know them ?- rather just a concentric tube.? Glass pump plans seem to be more geared to what is possible in glass working while the metal ones are geared to what is easy to turn or spin rather than what may be 'best'.? Which all seems to indicate that there are no magical dimensions.
?
If anyone else has more info on actual dimensions and construction of a diff pump, I am all ears.
?
Peter Smith.
?
?


More questions about oil diffusion pumps

 

Peter John Smith put a picture on his website of the internal construction of a vacuum
pump. It has helped but I don't think I understand and the drawing is not clear enough. I
also had a really good look at the picture of the glass pump. Please correct me if I am
using incorrect terminology.

Now for the questions.

How critical are the tolerances of the jet openings? The glass pump seems to have
quite big openings. Are the angles exceptionally critical? perpendicular will not work. I
assume that the angle has to be in the direction of flow as much as possible

How is the oil kept out of the pipe to the roughing pump? Or possibly a better question
is; how is the internal connection to the roughing pump normally made? The rough
drawing that the glass blower showed me had a collection chamber fed by a pipe to the
vaporisation chamber that sat below it. The glass pump picture just shows a pipe
exiting the chamber with possibly a connection to the lowest jet.

How does a fractionating pump work. Is it just the height of the assembly as is normally
done with fractional distillation? Which means any pump with jets at different heights
will be a fractionating pump.

Does the whole jet assembly fit in the body loosely or is it secured in?

Are each of the jets fed separately or are all the jets fed from the same tube? The glass
pump seems as if all are fed separately but the pump Peter John Smith showed seems
to have one tube. Is this the difference between a fractionating and non fractionating
pump?

I am sure I will think of some more questions to ask but I'll give you guys a break for
now.

Thanks

Geoff


Re: Digest Number 72

Gomez
 

On Monday, November 10, 2003, at 11:17 AM, nano_tronics wrote:

OK found it :)
The web site for this publication (The Bell Jar) can be found here:


You can even buy printed back-issue collections.